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JUNE 2022

DEVELOPMENT AND VALIDATION OF FT-IR SPECTROPHOTOMETRIC METHOD FOR SIMULTANEOUS ESTIMATION OF DICLOFENAC SODIUM AND RABEPRAZOLE SODIUM IN TABLET DOSAGE FORM

Anitha K^*¹, N. T. Rangari², T.M. Kalyankar³ and V. Y. Patil³

¹Department of Chemistry, Sri Krishnadevaraya University, Ananthapuram - 515003, Andhra Pradesh, India.

²KJs Educational Institute, Trinity College of Pharmacy, Yewalewadi, Pune-411048 Maharashtra, India.

³Department of Quality Assurance, School of Pharmacy, S. R. T. M. University, Vishnupuri, Nanded, Maharashtra 431606, India.

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FT-IR Spectrophotometric Method for Simultaneous Estimation of Atorvastatin calcium and Clopidogrel bisulphatein Combined Dosage Form

Anitha K^*¹, N. T. Rangari², T.M. Kalyankar³ and R.V. Birajdar³

¹Department of Chemistry, Sri Krishnadevaraya University, Ananthapuram - 515003, Andhra Pradesh, India.

²KJs Educational Institute, Trinity College of Pharmacy, Yewalewadi, Pune-411048 Maharashtra, India.

³Department of Quality Assurance, School of Pharmacy, S. R. T. M. University, Vishnupuri, Nanded, Maharashtra 431606, India.

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SIMULTANEOUS SPECTROPHOTOMETRIC ESTIMATION OF ISONIAZID AND PYRIDOXINE

Anitha K*1, T. M. Kalyankar2, U. A. Khedkar2, R. B. Gholve2
1Department of Chemistry, Sri Krishnadevaraya University, Ananthapuram - 515003, Andhra Pradesh, India.

2School of Pharmacy, Swami Ramanand Teerth Marathwada University, Nanded - 431606, Maharashtra, India.

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SIMULTANEOUS DETERMINATION OF METFORMIN AND GLIBENCLAMIDE IN PHARMACEUTICAL PREPARATION BY RP-HPLC

Anitha K¹, T. M. Kalyankar², V. B. Ingale² and Ashok P Gingine³

¹Department of Chemistry, Sri Krishnadevaraya University, Ananthapuram-515003, Andhra Pradesh, India.

²School of Pharmacy, Swami Ramanand Teerth Marathwada University, Nanded (431 606), MS India.

³School of Educational Sciences, Swami Ramanand Teerth Marathwada University, Nanded (431 606), MS India.

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A VALIDATED RP- HPLC METHOD FOR SIMULTANEOUS ESTIMATION OF ARTESUNATE, SULFADOXINE AND PYRIMETHAMINE IN BULK AND TABLETS FORMULATION

Anitha K¹, T. M. Kalyankar², Khan Jawad S. A.² and Ashok P Gingine³
¹Department of Chemistry, Sri Krishnadevaraya University, Ananthapuram-515003, Andhra Pradesh, India.
²School of Pharmacy, Swami Ramanand Teerth Marathwada University, Nanded (431 606), MS India.
³School of Educational Sciences, Swami Ramanand Teerth Marathwada University, Nanded (431 606), MS India.

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UV SPECTROPHOTOMETRIC METHOD FOR THE ESTIMATION OF TERIFLUNOMIDE IN TABLET.

M. S. Kalshetti^*, Vidyasree Kumbhar, Priti Reure, Shraddha Jamakhandi

Dept. of Pharmaceutical Quality Assurance, D.S.T.S Mandal’s College of Pharmacy, Solapur.

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DEVELOPMENT AND VALIDATION OF UV SPECTROPHOTOMETRIC METHOD FOR ESTIMATION OF SIROLIMUS IN TABLET.

M. S. Kalshetti*, Priti Reure, Vidyashree Kumbhar, Shraddha Jamakhandi

Dept of Pharmaceutical Quality Assurance, D.S.T.S. Mandal's College of Pharmacy, Solapur.

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MICRONEEDLE: AN OVERVIEW

Babar Sonali S.*, BarboleSadhana C., PatoleMayur M., KhumbharNikita A., Gidde Nikita D.

Adarsh College of Pharmacy, Vita. (MS) India.

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TO ASSESS THE APPROPRIATE DOSING OF ANTIMICROBIALS, ANTIHYPERTENSIVES AND ORAL HYPOGLYCEMIC AGENTS IN CHRONIC KIDNEY DISEASE PATIENTS AT TERTIARY CARE HOSPITAL: A RETROSPECTIVE, OBSERVATIONAL STUDY

Dr. Pankaj Shirsath¹, Richa P. Patel¹, Fatmabibi S. Tadwala¹, Khushboo M. Patel¹, Dr. Kalpesh Gohel²

¹Shree Dhanvantary Pharmacy College, Kim, Surat, Gujarat – 394111.

²Kiran Multi Super Speciality Hospital, Surat,Gujarat – 395004.

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ORAL CONTROLLED RELEASE AND TASTE MASKED SUSPENSION OF CEPHALEXIN USING ION EXCHANGE RESIN

Monica RP. Rao*, Suhen N. Chutake, Madhura R. Patil, Saloni A. Sakharwade

AISSMS College of Pharmacy, Kennedy Road, Near R.T.O, Pune-411001, Maharashtra, India.

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ENHANCEMENT OF BIOAVAILABILITY OF POORLY WATER-SOLUBLE DRUG BY SOLID SMEDDS.

Monica RP. Rao*, Amruta S. Badhe, Jidnyasa Pawar, Sushant Deshpande, Omkar Kudumble

AISSMS College of Pharmacy, Pune-411001, India.

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Lecardipine HCl (LCD) is a highly lipophilic dihydropyridine calcium antagonist indicated for the treatment of mild to moderate hypertension. It has poor aqueous solubility (less than 5 µg/ml) and its oral bioavailability is around 10%. The primary objectives of the present work was to develop, optimize and characterize the composition of a stable liquid and solid self-micro emulsifying drug delivery system (SMEDDS) of LCD HCl and to evaluate its oral bioavailability in rats. The LCD SMEDDS was prepared using Capmul MCM L8 (oil), Cremophor ELP (surfactant), and propylene glycol (cosurfactant). Liquid SMEDDS were converted to solid SMEDDS by adsorbing it on inert solid carrier. Flow properties were determined and solid-state characterization was done by SEM, DSC and XRPD. Optimized formulation showed complete release within 60 min. Stability study was done to check any drug precipitation or instability. HPTLC method was used to interpret in vivo studies of solid SMEDDS in rats. Area under curve and time were compared with those of pure drug suspended in 1% CMC solution. The area under curve and time showed significant improvement as the values obtained were 7680.19 ng h/ml and 1h for SMEDDS in comparison to 3574. 191 ng h/ml and 1.5 h for pure drug suggesting significant increased in oral bioavailability of SMEDDS of LCD HCl.Lecardipine HCl (LCD) is a highly lipophilic dihydropyridine calcium antagonist indicated for the treatment of mild to moderate hypertension. It has poor aqueous solubility (less than 5 µg/ml) and its oral bioavailability is around 10%. The primary objectives of the present work was to develop, optimize and characterize the composition of a stable liquid and solid self-micro emulsifying drug delivery system (SMEDDS) of LCD HCl and to evaluate its oral bioavailability in rats. The LCD SMEDDS was prepared using Capmul MCM L8 (oil), Cremophor ELP (surfactant), and propylene glycol (cosurfactant). Liquid SMEDDS were converted to solid SMEDDS by adsorbing it on inert solid carrier. Flow properties were determined and solid-state characterization was done by SEM, DSC and XRPD. Optimized formulation showed complete release within 60 min. Stability study was done to check any drug precipitation or instability. HPTLC method was used to interpret in vivo studies of solid SMEDDS in rats. Area under curve and time were compared with those of pure drug suspended in 1% CMC solution. The area under curve and time showed significant improvement as the values obtained were 7680.19 ng h/ml and 1h for SMEDDS in comparison to 3574. 191 ng h/ml and 1.5 h for pure drug suggesting significant increased in oral bioavailability of SMEDDS of LCD HCl.

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Lecardipine HCl (LCD) is a highly lipophilic dihydropyridine calcium antagonist indicated for the treatment of mild to moderate hypertension. It has poor aqueous solubility (less than 5 µg/ml) and its oral bioavailability is around 10%. The primary objectives of the present work was to develop, optimize and characterize the composition of a stable liquid and solid self-micro emulsifying drug delivery system (SMEDDS) of LCD HCl and to evaluate its oral bioavailability in rats. The LCD SMEDDS was prepared using Capmul MCM L8 (oil), Cremophor ELP (surfactant), and propylene glycol (cosurfactant). Liquid SMEDDS were converted to solid SMEDDS by adsorbing it on inert solid carrier. Flow properties were determined and solid-state characterization was done by SEM, DSC and XRPD. Optimized formulation showed complete release within 60 min. Stability study was done to check any drug precipitation or instability. HPTLC method was used to interpret in vivo studies of solid SMEDDS in rats. Area under curve and time were compared with those of pure drug suspended in 1% CMC solution. The area under curve and time showed significant improvement as the values obtained were 7680.19 ng h/ml and 1h for SMEDDS in comparison to 3574. 191 ng h/ml and 1.5 h for pure drug suggesting significant increased in oral bioavailability of SMEDDS of LCD HCl.Lecardipine HCl (LCD) is a highly lipophilic dihydropyridine calcium antagonist indicated for the treatment of mild to moderate hypertension. It has poor aqueous solubility (less than 5 µg/ml) and its oral bioavailability is around 10%. The primary objectives of the present work was to develop, optimize and characterize the composition of a stable liquid and solid self-micro emulsifying drug delivery system (SMEDDS) of LCD HCl and to evaluate its oral bioavailability in rats. The LCD SMEDDS was prepared using Capmul MCM L8 (oil), Cremophor ELP (surfactant), and propylene glycol (cosurfactant). Liquid SMEDDS were converted to solid SMEDDS by adsorbing it on inert solid carrier. Flow properties were determined and solid-state characterization was done by SEM, DSC and XRPD. Optimized formulation showed complete release within 60 min. Stability study was done to check any drug precipitation or instability. HPTLC method was used to interpret in vivo studies of solid SMEDDS in rats. Area under curve and time were compared with those of pure drug suspended in 1% CMC solution. The area under curve and time showed significant improvement as the values obtained were 7680.19 ng h/ml and 1h for SMEDDS in comparison to 3574. 191 ng h/ml and 1.5 h for pure drug suggesting significant increased in oral bioavailability of SMEDDS of LCD HCl.

A REVIEW ON NASAL DRUG DELIVERY: OPPORTUNITIES AND CHALLENGES

Neha Kandpal*, Shaffi Tangri

School of Pharmaceutical Science, Shri Guru Ram Rai University, Dehradun, India.

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A REVIEW ON ORAL DISPERSIBLE TABLET (ODT).

Shreyansh Prajapati, Atmiy Patel, Rahul Sonkar, Ankur Ninama, Ajay Dhoom

Shivam Pharmaceutical Studies & Research Centre, Valasan, Anand, Gujarat.

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DEVELOPMENT OF GREEN TEA AQUEOUS EXTRACT LOADED CHITOSAN MEMBRANE FOR WOUND HEALING AND ITS EFFECT IN CONTROLLING NOSOCOMIAL INFECTION.

Shilpa J^* and Jayachandran VP^#

Department of Biotechnology, Sri Shakthi Institute of Engineering and Technology, Coimbatore, Tamil Nadu, India.

Department of Applied Sciences, University of Technology and Applied Sciences, PO Box 74, Al-Khuwair, Postal Code- 133.

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A GREEN CURE FOR ALZEIMERS DISEASE: A CRITICAL REVIEW

Nidhi Patel^*, Divyang Patel, Tejas Patel

Pioneer Pharmacy Degree College, Vadodara, Gujarat, India -390019.

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FORMULATION AND INVITRO EVALUATION OF DOXORUBICIN SUSTAINED RELEASE AND PALANOSETRON IMMEDIATE RELEASE LAYER IN BILAYER TABLET

Sk.Naheed¹, Shaik Nagulmeera², M.Upendar¹

¹Teja College of Pharmacy, Kodad-508206.

²Sana College of Pharmacy, Kodad-508206.

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DESIGN AND EVALUATION OF TASTE MASKED DRUG RESIN COMPLEX (DRC) OF FLUCONAZOLE

Vani Madaan^*1, Mahesh Kumar Kataria², Ajay Bilandi³

Arya College of Pharmacy, Jaipur, India. Department Pharmaceutics, Seth G.L. Bihani S.D.

College of Technical Education, Sri Ganganagar, Rajasthan.

College of Pharmacy, RIMT University, Mandi Gobingarh, Punjab.

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FORMULATION AND EVALUATION OF EXTRACTED PEARL MILLET STARCH AS TABLET DISINTEGRANT IN DICLOFENAC SODIUM TABLET PREPARATION

Amit Kumar Tiwari^*, S.A. Sreenivas

Mewar University, Gangrar, Chittorgarh, Rajasthan.

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Objectives: This study aims to evaluate a novel tablet excipient obtained from local sources, Pearl millet Pannistum americanum starch of family Poaceae which is used locally as food because of its high carbohydrate content. It was thought that the starch of Pearl millet Pannistum americanum may serve as a tablet disintegrant. Methods: The excipient properties of Pearl millet starch as well as the pregelatinized form were studied in paracetamol tablets produced by wet and dry granulation methods of massing and screening and compared with maize starch BP.Results: Wet method showed superiority in all properties of both granules and tablets. Using wet method granulations Pearl millet Pannistum americanum starch and maize starch BP have similar angle of repose, Carrs index, tapped density, bulk density, and Hausners ratio, however, Pearl millet Pannistum americanum starch has shown advantageous in some properties such as moisture content and swelling index. Tablet produced with Pearl millet Pannistum americanum starch disintegrated almost the same of those produced with maize starch BP at all concentrations employed. It was also found that when used as a disintegrant, the pre-gelatinized form provide tablets with better hardness and friability values than maize starch BP.Conclusion: This study confirmed the suitability of Pearl millet Pannistum americanum starch as an alternative to maize starch BP as a tablet disintegrant, particularly, in Diclofenac sodium tablet formulation.

Objectives: This study aims to evaluate a novel tablet excipient obtained from local sources, Pearl millet Pannistum americanum starch of family Poaceae which is used locally as food because of its high carbohydrate content. It was thought that the starch of Pearl millet Pannistum americanum may serve as a tablet disintegrant. Methods: The excipient properties of Pearl millet starch as well as the pregelatinized form were studied in paracetamol tablets produced by wet and dry granulation methods of massing and screening and compared with maize starch BP.Results: Wet method showed superiority in all properties of both granules and tablets. Using wet method granulations Pearl millet Pannistum americanum starch and maize starch BP have similar angle of repose, Carrs index, tapped density, bulk density, and Hausners ratio, however, Pearl millet Pannistum americanum starch has shown advantageous in some properties such as moisture content and swelling index. Tablet produced with Pearl millet Pannistum americanum starch disintegrated almost the same of those produced with maize starch BP at all concentrations employed. It was also found that when used as a disintegrant, the pre-gelatinized form provide tablets with better hardness and friability values than maize starch BP.Conclusion: This study confirmed the suitability of Pearl millet Pannistum americanum starch as an alternative to maize starch BP as a tablet disintegrant, particularly, in Diclofenac sodium tablet formulation.

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Objectives: This study aims to evaluate a novel tablet excipient obtained from local sources, Pearl millet Pannistum americanum starch of family Poaceae which is used locally as food because of its high carbohydrate content. It was thought that the starch of Pearl millet Pannistum americanum may serve as a tablet disintegrant. Methods: The excipient properties of Pearl millet starch as well as the pregelatinized form were studied in paracetamol tablets produced by wet and dry granulation methods of massing and screening and compared with maize starch BP.Results: Wet method showed superiority in all properties of both granules and tablets. Using wet method granulations Pearl millet Pannistum americanum starch and maize starch BP have similar angle of repose, Carrs index, tapped density, bulk density, and Hausners ratio, however, Pearl millet Pannistum americanum starch has shown advantageous in some properties such as moisture content and swelling index. Tablet produced with Pearl millet Pannistum americanum starch disintegrated almost the same of those produced with maize starch BP at all concentrations employed. It was also found that when used as a disintegrant, the pre-gelatinized form provide tablets with better hardness and friability values than maize starch BP.Conclusion: This study confirmed the suitability of Pearl millet Pannistum americanum starch as an alternative to maize starch BP as a tablet disintegrant, particularly, in Diclofenac sodium tablet formulation.

Objectives: This study aims to evaluate a novel tablet excipient obtained from local sources, Pearl millet Pannistum americanum starch of family Poaceae which is used locally as food because of its high carbohydrate content. It was thought that the starch of Pearl millet Pannistum americanum may serve as a tablet disintegrant. Methods: The excipient properties of Pearl millet starch as well as the pregelatinized form were studied in paracetamol tablets produced by wet and dry granulation methods of massing and screening and compared with maize starch BP.Results: Wet method showed superiority in all properties of both granules and tablets. Using wet method granulations Pearl millet Pannistum americanum starch and maize starch BP have similar angle of repose, Carrs index, tapped density, bulk density, and Hausners ratio, however, Pearl millet Pannistum americanum starch has shown advantageous in some properties such as moisture content and swelling index. Tablet produced with Pearl millet Pannistum americanum starch disintegrated almost the same of those produced with maize starch BP at all concentrations employed. It was also found that when used as a disintegrant, the pre-gelatinized form provide tablets with better hardness and friability values than maize starch BP.Conclusion: This study confirmed the suitability of Pearl millet Pannistum americanum starch as an alternative to maize starch BP as a tablet disintegrant, particularly, in Diclofenac sodium tablet formulation.

A STUDY ON DRUG PRESCRIBING PATTERN, DRUG INTERACTION AND EVALUATION OF MEDICATION ADHERENCE AMONG SMOKING AND NON-SMOKING CHRONIC OBSTRUCTIVE PULMONARY DISEASE PATIENTS IN TERTIARY CARE TEACHING HOSPITAL

Anupriya Jose¹, Sonu Maria Sojan¹, Sinha Ritesh¹, T. Chaithanya Kumar²

¹Department of Pharmacy Practice, SET’s College of Pharmacy, Dharwad, Karnataka, India.

²Assistant Professor, Department of Pharmacy Practice, SET’s college of pharmacy, Dharwad Karnataka, India.

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RECENT ADVANCES IN POLYMERIC DRUG DELIVERY SYSTEM

ShitalMisal^*. Shilpa Shiragave, Jaydeep Pawar

HSBPVT’s, GOI, College of Pharmacy, Kashti, MH, India, 414701.

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EVALUATION OF ANTI-HYPERTENSIVE DRUG PRESCRIPTION PATTERN ACCORDING TO JOINT NATIONAL COMMITTEE-8, ASSESSMENT OF MEDICATION ADHERENCE AND DRUG RELATED PROBLEM IN TYPE-2 DIABETES MELLITUS PATIENTS

Jemy Jose, Muneer A, Mannu Jaiswar, Dr. Apurva Edward Pilli

SET’s college of Pharmacy, Dharwad Karnataka-580002, India.

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MOLECULAR DOCKING STUDIES OF SOME NOVEL PYRROLYL PYRAZOLE DERIVATIVES.

Sandhya Chinnamulagund, Shrinivas D. Joshi^*, Channabasappa S. Hallikeri, Ashwini Joshi, Venkatrao H. Kulkarni

Soniya Education Trust’s College of Pharmacy, Sangolli Rayanna Nagar, Dharwad 580 002, Karnataka, India.

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DEVELOPMENT AND VALIDATION OF STABILITY INDICATING DENSITOMETRIC METHOD FOR ESTIMATION OF APREMILAST IN BULK DRUG AND TABLET DOSAGE FORM

Padmanabh B. Deshpande*, Snehal R. Dhamodkar, Sushant Deshpande, Nutan Raut

All India Shri Shivaji Memorial Society’s College of Pharmacy, Department of Pharmaceutical Quality Assurance, Kennedy Road, Near RTO, Pune-411001.

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PRODUCTION AND OPTIMIZATION OF PECTINASE BY STAPHYLOCOCCUS AUREUS. ISOLATED FROM ORANGE PEEL WASTE

Mevada Krupal Rajendrakumar¹, PrajapatiDhaval Dineshbhai²

Shree Kumarbhai Sevantilal Javeri Science College, Vimla Vidhyalaya, Gadh.

Mehsana Urban Institute of Science, Ganpat University, Mehsana.

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FLORA OF MEDICINAL PLANTS IN JSSAC, MYSURU

Tejashwini Hiremath, Pooja, N., Kiran, B. L.

JSS College of Arts, Science and Commerce, Mysore- 570025. INDIA.

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CRUDE COUMARIN EXTRACT PREPARATION USING CASSIA CINNAMON POWDER AND ITS pH ANALYSIS WITH EXAMINATION OF ANTIMICROBIAL ACTIVITY

Ganesh Gautam Verma^*, Mrs. Suvarna Patil, Kajal Rane

Ideal College of Pharmacy & Research- Mumbai University.

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MEDICINAL PROPERTIES, PHYTOCHEMISTRY AND PHARMACOLOGY OF ARISTOLOCHIA ROTUNDA LINN: A POTENT UNANI DRUG

Dr. Syeda Sumaiya^1*, Prof. Wajeeha Begum¹, Dr. Ghufran Najeeb3, Dr. Shabnam Bano¹.

¹Dept of Ilmul Qabalat wa Amraze Niswan, National Institute of Unani Medicine, Bangalore-91, Karnataka, India.

²Unani Medical Officer, Dept of public health, Ministry of H & FW Govt of Chhattisgarh.

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FORMULATION AND EVALUATION OF HERBAL CREAM OF EUCALYPTUS GLOBULUS AND ALOE BARBIDENSE LEAVES EXTRACT FOR ANTI-ACNE ACTIVITY

Rajesh Akki^1*, Munagala Gayatri Ramya², Vardhani1, Singaram Kathirvel³

¹Hindu College of Pharmacy, Guntur 522 002.

²University College of Pharmaceutical Sciences, Nagarjuna Nagar – 522 510.

³National College of Pharmacy, Kozhikode 673572.

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POSTMENOPAUSAL SYNDROME AND THEIR MANAGEMENT

Himanshi, Sandeep Singh

School of Pharmaceutical Sciences, Jaipur National University, Jaipur-302017, India.

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PHYTOCHEMICAL SCREENING AND IN-VITRO ANTIOXIDANT PROPERTY OF POLYHERBAL MIXTURE OF RUBIA CORDIFOLIA, VITEX NEGUNDO, PIPER NIGRUM, MYRISTICA FRAGRANS

Sapna Desai^*, Ankita Desai, Komal Rahevar, Divyang Patel, Dipal Prajapati

Department of Pharmacy, Pioneer Pharmacy Degree College, Vadodara, Gujarat, India -390019.

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